Focuses on magnetic resonance methods for characterizing solid carbonaceous fuels. Covers 2-D methods, high-resolution ¹³C and ¹H NMR (CRAMPS) analyses, dynamic nuclear polarization techniques, temperature-dependent relaxation measurements, chemical methods to improve quantitative reliability, ultrafast MAS methods, and new signal enhancement techniques. Discusses topics of current interest in the areas of ESR, including spin-echo methods, 1-D and 2-D pulses EST techniques, relaxation time measurements, and ultrahigh frequency measurements. Measurements are made on a set of Argonne Premium Coal samples to compare different magnetic resonance techniques on a homogeneous set of carbonaceous fuel samples.
Edited by:
Robert E. Botto,
Yuzo Sanada
Imprint: American Chemical Society
Country of Publication: United States
Volume: 229
Dimensions:
Height: 234mm,
Width: 158mm,
Spine: 35mm
Weight: 965g
ISBN: 9780841218666
ISBN 10: 0841218668
Series: Advances in Chemistry Series
Pages: 666
Publication Date: 01 January 1993
Audience:
Professional and scholarly
,
Undergraduate
Format: Hardback
Publisher's Status: Active
R.A. Wind, G.E. Maciel, and R.E. Botto: Quantitation in ¹³C NMR Spectroscopy of Carbonaceous Solids G.E Maciel, C.E. Bronnimann, and C.F. Ridenour: ¹H NMR Spectroscopy: Approaches for Carbonaceous Solids R.A. Wind, R. Lewis, H. Lock, and G.E. Maciel: Solid Materials Research with NMR and Dynamic Nuclear Polarization Spectroscopy H. Thomann and M. Bernardo: Advances in Electron Nuclear Double Resonance Spectroscopy M.K. Bowman: Strategies for Measurement of Electron Spin Relaxation R.L. Belford and R.B. Clarkson: Multifrequency Electron Paramagnetic Resonance Spectroscopy Y. Sanada and L.J. Lynch: High-Temperature Electron Spin Resonance and NMR Methods Applied to Coal W.A. Barton, L.J. Lynch, D.S. Webster, and G. Simms: Diffusion-Coupled Relaxation and the Submicroscopic Structure of Bituminous Coals A.M. Vassallo: ¹³C NMR Spectroscopy of Pyridine and Alkylpyridines Sorbed onto Coal R.A. Wind: Distortion-Free ¹³C NMR Spectroscopy in Coal: ¹H Rotating-Frame Dynamic Nuclear Polarization and ¹H-¹³C Cross-Polarization R. Sakurovs, L.J. Lynch, and W.A. Barton: Proton Magnetic Resonance Thermal Analysis of Argonne Premium Coals D.E. Axelson: Multivariate Statistical Analysis and Pattern Recognition: Principal-Component Analysis of Coal Solid-State NMR Relaxation Times Y. Adachi and M. Nakamizo: Structural Parameters of Argonne Coal Samples: Solid-State ¹³C NMR Spectroscopy N. Cyr and N.O. Egiebor: Characterization of Coal Liquefaction Residues by Solid-State ¹³C NMR Spectroscopy K. Hayamizu, S. Hayashi, K. Kamiya, and M. Kawamura: ¹H NMR Spectroscopy and Spin-Lattice Relaxation of Argonne Premium Coals J. Hu, L. Li, and C. Ye: High-Field NMR Studies of Argonne Premium Coals J.A. MacPhee, H. Kawashima, Y. Yamashita, and Y. Yamada: Solid-State ¹³C NMR Studies on Coal and Coal Oxidation C. Tsiao and R.E. Botto: Measurement of Spin-Lattice Relaxation in Argonne Premium Coal Samples L. dela Rosa, M. Pruski, and B. Gerstein: Quantitation of Protons in the Argonne Premium Coals by Solid-State ¹H NMR Spectroscopy J.A. Franz and J.C. Linehan: Bloch-Decay and Cross-Polarization--Magic-Angle Spinning ¹³C NMR Study of the Argonne Premium Coals: Effects of High-Speed Spinning A. Jurkiewicz, C. E. Bronnimann, and G.E. Maciel: High-Resolution ¹H NMR Studies of Argonne Premium Coals A.M. Orendt, M.S. Solum, N.K. Sethi, C.D. Hughes, R.J. Pugmire, and D.M. Grant: Measurement of ¹³C Chemical-Shift Anisotropy in Coal Y.D. Tsvetkov, S.A. Dzuba, and V.I. Gulin: 2-mm Band and X-Band Electron Spin Resonance and Electron Spin Echo Investigations of Some Carbonaceous Materials X. Chen, H. McManus, and L. Kevan: Electron Spin Resonance, Electron Nuclear Double Resonance, and Electron Spin Echo Spectroscopic Studies of Argonne Premium Coals R. Spears, J. Goslar, and L.D. Kispert: Electron Paramagnetic Resonance Spin-Probe Studies of Porosity in Solvent-Swelled Coal H.A. Buckmaster and J. Kudynska: Dynamic In Situ 9-GHz Electron Paramagnetic Resonance Studies of Argonne Premium Coal Samples R.B. Clarkson, W. Wang, D.R. Brown, H.C. Crookham, and R.L. Belford: Electron Magnetic Resonance of Standard Coal Samples at Multiple Microwave Frequencies T. Keneko, M. Sasaki, T. Yokono, and Y. Sanada: Novel Characterization of Argonne Premium Coals with Electron Donors or Acceptors by Electron Paramagnetic Resonance Spectroscopy B.G. Silbernagel, L.A. Gebhard, M. Bernardo, and H. Thomann: Electron Paramagnetic Resonance and Electron Spin Echo Spectroscopy of Argonne Premium Coals H. Thomann, M. Bernardo, and B. G. Silbernagel: Pulsed Electron Nuclear Double Resonance Spectroscopy of Argonne Premium Coals K.S. Rothenberger, R.F. Sprecher, S.M. Castellano, and H.L. Retcofsky: Temperature Dependence of the Electron Paramagnetic Resonance Intensity of Whole Coals: The Search for Triplet States M.K. Bowman: Measurement of Electron Dipolar Fields and Dynamics in Solids B.G. Silbernagel and R.E. Botto: Advanced Magnetic Resonance Techniques Applied to Argonne Premium Coals
