Experimental Methods in Organic Fluorine Chemistry

Tomoya Kitazume, Takashi Yamazaki

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English

CRC Press
02 December 2019

Inorganic chemistry; Organic chemistry

In the fields of biologically active materials and functional materials, fluorinated organic materials are becoming a focus of significant interest. Over the past decade synthetic methodologies and reagents in fluorine chemistry have been developed, especially stereocontrolled synthetic methods, enzymatic resolution to synthesize enantiomers, fluoromethylated reagents, and fluorination reagents. These methods have contributed to the opening of new pathways for fluorinated materials. However, few fluorinated materials have been put to commercial use. Furthermore, there remain problems to be solved, such as the handling of the materials, availability of reagents and selectivity (stereo-, regio-, and/or chemoselectivity). Research chemists, technical engineers, and graduate students in all branches of chemistry, pharmaceutics, and material science interested in fluorinated materials need to know detailed experimental procedures of how to synthesize the target fluorinated materials.

This volume summarizes the chemical and microbial methods for obtaining functionalized fluorinated materials for use as building blocks; detailed experimental methods (reaction conditions, solvent, temperature, handling techniques, etc.); and the stereoview (possible absolute configuration) of the structures with spectral data. Mono-, di-, tri-, and polyfluorinated materials derived from fluorinating agents, fluoromethylated reagents and building blocks are summarized. A chemical name index, molecular formula index, and reagent index are also included. The publication of this monograph will provide access to the enormous possibilities in fluorine chemistry, biological material chemistry, and functionalized material chemistry.

By: Tomoya Kitazume, Takashi Yamazaki
Imprint: CRC Press
Country of Publication: United Kingdom
Dimensions: Height: 246mm, Width: 174mm,
Weight: 453g
ISBN: 9780367455668
ISBN 10: 0367455668
Pages: 272
Publication Date: 02 December 2019
Audience: College/higher education , Professional and scholarly , Further / Higher Education , Undergraduate
Format: Paperback
Publisher's Status: Active

1. Effect of Fluorine on Physical Properties 2. Preparation of Fluorine-containing Materials 3. Handling Fluorinated Materials 4. Fluorination 5. Carbon-Carbon Bond-forming Reactions 6. Removal of Fluorine from Difluorinated Materials 7. Difluoromethylenation 8. Introduction of a Trifluoromethyl Group 9. Reactions with Hetero Nucleophiles 10. Effect of Fluorine on Chemical Reactivity 11. Oxidations and Reductions 12. Optical Resolutions 13. Introduction of Poly- or Perfluorinated Groups

Tomoya Kitazume, associate professor of bioengineering, and Takashi Yamazaki, researcher of bioengineering, are both members of Tokyo Institute of Technology.